Advanced organic synthesis : a laboratory manual

Description

Diastereoselective Reduction of EstroneEquipment RequiredMaterials RequiredOverall ReactionProcedureReferencesSynthesis of 2,2-Dimethyl-4-pentene-1-amineEquipment RequiredMaterials RequiredOverall ReactionProcedureReferencesProtection of 2,2-Dimethyl-4-pentene-1-amineEquipment RequiredMaterials RequiredOverall ReactionProcedureReferencesOptimization of the Reaction Conditions for the Aminofluorination of N-(2,2-Dimethylpent-4-enyl)-2-toluenesulfonamideEquipment RequiredMaterials RequiredProcedureReferencesAsymmetric Robinson AnnulationEquipment RequiredMaterials RequiredOverall ReactionProcedureReferencesFormation of N-Benzylcinchonidinium Chloride from CinchonidineEquipment RequiredMaterials RequiredOverall ReactionProcedureChiral Resolution of BINOL (1,1'-bi-2-Naphthol) with N-Benzylcinchonidinium ChlorideEquipment RequiredMaterials RequiredOverall ReactionProcedureReferencesTransesterification of Phosphatidylcholine and FAME QuantificationEquipment RequiredMaterials RequiredOverall ReactionProcedureReferencesGreen Chemistry: Solventless Sequential Aldol and Michael Reactions in the Synthesis of Kroehnke PyridineEquipment RequiredMaterials RequiredOverall ReactionProcedureReferencesCarbonyl Chemistry in a Multistep SynthesisEquipment RequiredMaterials RequiredOverall ReactionProcedureReferencesMultistep Synthesis of a Bioactive PeptidomimeticEquipment RequiredMaterials RequiredStock SolutionsOverall ReactionProcedureReferencesTotal Synthesis of a Natural Product: Caffeic Acid Phenethyl Ester (CAPE)Equipment RequiredMaterials RequiredOverall ReactionProcedureReferencesAppendix: Essential Laboratory TechniquesChoosing GlasswareDrying GlasswarePurging with Inert GasSetting a Pressure Release ValveHandling of Pyrophoric and Water-Sensitive ReagentsSetting Up a Chromatography ColumnPulling SpottersSpotting and Running a TLC PlateDry Solvents and ReagentsSetting Up an Apparatus