Practical Pharmaceutical Organic Chemistry I & II for Second and Third Semesters Bachelors of Pharmacy
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Front Cover Half Title Title Copyright Preface Contents Part I: Practical Pharmaceutical Organic Chemistry Course Code: BP208P 1. Introduction 1. General Laboratory Techniques 2. Crystallization and Recrystallization 3. Extraction 4. Chromatography 2. Hydrocarbons Saturated Hydrocarbons (Alkanes) Unsaturated Hydrocarbons (Alkenes and Alkynes) Functional Groups Tests for Unsaturation 3. Lassaigne‘s Extract (Sodium Fusion Extract) 4. Functional Group Tests Tests for Alcoholic Group Tests for Alcohol Tests for Esters Tests for Phenolic Group Tests for Phenols Tests for Aldehydic and Ketonic Groups Tests for Carboxylic Group: Aldehyde and Ketone Tests for Carboxylic Acid Tests for Carboxylic Groups Tests for Carbohydrates Tests for Amines Tests for Anilides Test for Nitroso Group 5. Identification of Organic Compound by Organic Qualitative Analysis 1. Preliminary Test 2. Solubility Test 3. Detection of Extra Elements 4. Detection of Functional Group 5. Determination of Physical Constant and Identification of the Compounds 6. Confirmatory Test 7. Derivatives Preparation and its Melting Point Determination 8. Carboxylic Acids 9. Alcohols 10. Phenols 11. Aldehydes and Ketones 12. Esters 13. Carbohydrates 14. Hydrocarbons 15. Amides 16. Amines 17. Anilides or Substituted Amides 18. Nitro Compound 19. Thioamide (Thiourea) 20. Acids 21. Identification of Unknown Compound Using Melting Point/Boiling Point and their Derivatives 6. Experiments Experiment 1: Study about Identification of Molecular or Ionic Determining of Organic Chemical Substance to Distinguish from other Compounds Experiment 2: To Identify Unknown Organic Compounds by the Preliminary Test (Nature, Colour and Odour) Experiment 3: To Identify Unknown Organic Compounds by the Ignition (Preliminary Tests) Experiment 4: To identify Unknown Organic Compounds by the Preliminary Tests (Test for Saturation and Unsaturation) Experiment 5: To Identify Nitrogen by Lassaigne’s Test from Unknown Organic Compounds Experiment 6: To Identify Sulphur by Lassaigne’s Test from Unknown Organic Compounds Experiment 7: To Identify Halogens by Lassaigne’s Test from Unknown Organic Compounds Experiment 8: To Perform Solubility Test in Given Unknown Organic Compounds Experiment 9: Detection of Functional Groups (Amides and Phenols) of Given Unknown Organic Compounds Experiment 10: Detection of Functional Groups (Carbohydrate and Amines) of Given Unknown Organic Compounds Experiment 11: Detection of Functional Groups (Carboxylic Acid, Aldehydes, Ketones) of Given Unknown Organic Compounds Experiment 12: Detection of Functional Groups (Alcohol and Esters) of Given Unknown Organic Compounds Experiment 13: Detection of Functional Groups (Anilides, Nitro Compoundsand Halogen Hydrocarbons) of Given Unknown Organic Compounds Determination of Melting Point Experiment 14: To Determine the Melting Point of Given Solid Substance Experiment 15: To Determine the Melting Point of Organic Compounds Like Naphthalene Experiment 16: To Determine the Melting Point of Organic Compounds Like Benzoic Acid Experiment 17: To Determine the Melting Point of Organic Compounds Like Sucrose Experiment 18: To Determine the Melting Point of Organic Compounds LikeIodine Experiment 19: To Determine the Melting Point of Organic Compounds Like Sodium Hydroxide Determination of Boiling Point Experiment 20: To Determine the Boiling Point of the Given Organic Compound Experiment 21: To Determine the Boiling Point of Organic Compounds Like Benzene Experiment 22: To Determine the Boiling Point of Organic Compounds Like Benzaldehyde Experiment 23: To Determine the Boiling Point of Organic Compounds Like Chloroform Experiment 24: To Determine the Boiling Point of Organic Compounds Like Distilled Water Experiment 25: To Determine the Boiling Point of Organic Compounds LikeIsopropyl Alcohol Experiment 26: To Analysis Organic Compound (Urea Nitrate) Experiment 27: To Analysis Organic Compound (Benzoate Derivative) Experiment 28: To Analysis Organic Compound (2,4-Dinitrophenyl Hydrazone) Experiment 29: To Analysis Organic Compound (Oxime Derivative) Experiment 30: To Analysis Organic Compound (Base Catalyzed Derivative) Experiment 31: To Analysis Organic Compound (Benzoate Derivative) by Schotten-Baumann Eeaction Construction of Molecular Models Experiment 32: To Study about Construction of Molecular Models for Unknown Organic Compound Experiment 33: To Construct the Molecular Models for Nitrogen Experiment 34: To Construct the Molecular Models for Oxygen 7. IUPAC Nomenclature of Organic Compounds Part II: Experimental Pharmaceutical Organic Chemistry II Course Code: BP305P 8. Experiments Recrystallization Experiment 1: Study About Recrystallization Experiment 2: To Purify the Given Organic Compounds by Recrystallization Steam Distillation Experiment 3: To Setup Assembly for Simple Distillation Experiment 4: To Study the Characteristics of Steam Distillation Experiment 5: To Purify the Mixture of Heptanes and Hexane by Distillation Acid Value Experiment 6: Determination of Acid Value of Oil Saponification Value Experiment 7: Method to Determine the Saponification Value of Oil Iodine Value Experiment 8: Method to Determine the Iodine Number Value of Oil Preparation of Compounds Experiment 9: To Prepare Benzanilide (N-benzyl Aniline) from aniline Experiment 10: To Prepare Phenyl Benzoate from Phenol Experiment 11: To Prepare the Organic Compound Acetanilide fromAniline Experiment 12: To Synthesize and Submit Aniline Experiment 13: To Prepare the Organic Compound 2,4,6-Tribromoanilinefrom Aniline Experiment 14: To Prepare the Organic Compound p-Bromoacetanilide Experiment 15: To Prepare the Organic Compound 5-Nitrosalicylic Acid Experiment 16: To Synthesize and Submit Nitrobenzene Experiment 17: To Prepare the Organic Compound Benzoic Acid from Benzyl Chloride Experiment 18: To Prepare the Organic Compound Salicylic Acid Experiment 19: To Prepare the Organic Compound 2-Naphthol Aniline Dyefrom Aniline Experiment 20: To Prepare the Organic Compound Benzil from Benzoin Experiment 21: To Prepare the Organic Compound Dibenzal Acetone from Benzaldehyde Experiment 22: To Prepare the Organic Compound p-Iodobenzoic Acid fromp-Aminobenzoic Acid Experiment 23: To Prepare the Organic Compound Cinnamic Acid fromBenzaldehyde Back Cover
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