Experimental Approaches of NMR Spectroscopy: Methodology and Application to Life Science and Materials Science
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This book describes the advanced developments in methodology and applications of NMR spectroscopy to life science and materials science. Experts who are leaders in the development of new methods and applications of life and material sciences have contributed an exciting range of topics that cover recent advances in structural determination of biological and material molecules, dynamic aspects of biological and material molecules, and development of novel NMR techniques, including resolution and sensitivity enhancement. First, this book particularly emphasizes the experimental details for new researchers to use NMR spectroscopy and pick up the potentials of NMR spectroscopy. Second, the book is designed for those who are involved in either developing the technique or expanding the NMR application fields by applying them to specific samples. Third, the Nuclear Magnetic Resonance Society of Japan has organized this book not only for NMR members of Japan but also for readers worldwide who are interested in using NMR spectroscopy extensively. Front Matter ....Pages i-xii Front Matter ....Pages 1-1 Protein Studies by High-Pressure NMR (Kazuyuki Akasaka)....Pages 3-36 Isotope-Aided Methods for Biological NMR Spectroscopy: Past, Present, and Future (Masatsune Kainosho, Yohei Miyanoiri, Mitsuhiro Takeda)....Pages 37-61 Advances in NMR Data Acquisition and Processing for Protein Structure Determination (Teppei Ikeya, Yutaka Ito)....Pages 63-90 Advances in High-Field DNP Methods (Yoh Matsuki, Toshimichi Fujiwara)....Pages 91-134 Photoirradiation and Microwave Irradiation NMR Spectroscopy (Akira Naito, Yoshiteru Makino, Yugo Tasei, Izuru Kawamura)....Pages 135-170 Solid-State NMR Under Ultrafast MAS Rate of 40–120 kHz (Yusuke Nishiyama)....Pages 171-195 Elucidating Functional Dynamics by R1ρ and R2 Relaxation Dispersion NMR Spectroscopy (Erik Walinda, Kenji Sugase)....Pages 197-225 Structural Study of Proteins by Paramagnetic Lanthanide Probe Methods (Tomohide Saio, Fuyuhiko Inagaki)....Pages 227-252 Structure Determination of Membrane Peptides and Proteins by Solid-State NMR (Izuru Kawamura, Kazushi Norisada, Akira Naito)....Pages 253-293 Front Matter ....Pages 295-295 NMR Studies on Silk Materials (Tetsuo Asakura, Yugo Tasei)....Pages 297-312 NMR Studies on Polymer Materials (Atsushi Asano)....Pages 313-339 Solid-State 2H NMR Studies of Molecular Motion in Functional Materials (Motohiro Mizuno)....Pages 341-364 NMR Spectral Observations of the Gases in Polymer Materials (Hiroaki Yoshimizu)....Pages 365-381 NMR Studies on Natural Product—Stereochemical Determination and Conformational Analysis in Solution and in Membrane (Nobuaki Matsumori, Michio Murata)....Pages 383-414 Technical Basis for Nuclear Magnetic Resonance Approach for Glycoproteins (Koichi Kato, Saeko Yanaka, Hirokazu Yagi)....Pages 415-438 NMR Studies on RNA (Taiichi Sakamoto, Maina Otsu, Gota Kawai)....Pages 439-459 NMR Analysis of Molecular Complexity (Jun Kikuchi)....Pages 461-489 NMR of Paramagnetic Compounds (Yasuhiko Yamamoto, Tomokazu Shibata)....Pages 491-518 NMR of Quadrupole Nuclei in Organic Compounds (Kazuhiko Yamada)....Pages 519-543 Quadrupole Nuclei in Inorganic Materials (Toshikazu Takahashi)....Pages 545-577 Protein–Ligand Interactions Studied by NMR (Hidekazu Hiroaki, Daisuke Kohda)....Pages 579-600 Protein Structure and Dynamics Determination by Residual Anisotropic Spin Interactions (Shin-ichi Tate)....Pages 601-636
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