ENGLISH

New Developments in Polymer Analytics I

By Schmidt M.

Book information

Publisher
Springer
Language
english
Format
PDF
Filesize
9 MB (9160285 bytes)
Series
Advanced in Polymer Science
Pages
\240
Time added
2021-11-27 23:03:59

Description

New Developmentsin Polymer Analytics I Volume Editor Editorial Board Preface Contents Hyphenated Techniques in Liquid Chromatography of Polymers Introduction Hyphenation in Polymer Analysis Hyphenation of Size Exclusion Chromatography with Selective Detectors General Considerations Coupling with Multiple Concentration Detectors Coupling with Molar-Mass-Sensitive Detectors Conclusions and Outlook Two-Dimensional Chromatography Orthogonal Chromatography Coupling of Liquid Adsorption Chromatography and SEC Coupling of Liquid Chromatography at the Critical Point of Adsorption and SEC Conclusions and Outlook Hyphenation of Liquid Chromatography with Spectroscopic Methods Coupling with FTIR Spectroscopy Coupling with Mass Spectroscopy Coupling with Proton NMR Conclusions and Outlook References Field-Flow Fractionation Techniques for Polymer and Colloid Analysis Introduction and Basic Principles History/The Family of Field-Flow-Fractionation (FFF) Techniques General Principles Accessible Quantities General Theoretical Considerations Elution in an FFF Channel Resolution, Theoretical Plate Heights and Peak Capacity Comparison of FFF with Other Analytical Techniques Comparison of FFF (Th-FFF and Fl-FFF) with SEC Comparison of FFF (Th-FFF and Fl-FFF) with Other Analytical Techniques Experimental Methodology General Equipment for FFF The FFF Experiment Relaxation Field Programming Optimization of the FFF Experiment FFF Techniques and Modes of Operation Sedimentation-FFF (S-FFF) Gravitational-FFF (Gr-FFF) Thermal-FFF (Th-FFF) Flow-FFF (Fl-FFF) Symmetrical Flow-FFF (S-Fl-FFF) Asymmetrical Flow-FFF (A-Fl-FFF) Electrical-FFF (El-FFF) Other Experimentally Tested FFF Techniques Magnetic-FFF Dielectrophoresis-FFF (DEP-FFF) Pressure-FFF Three-Dimensional Fl-FFF (Helical-Fl-FFF) Acoustic-FFF Photophoretic-FFF Theoretically Proposed FFF Techniques Concentration-FFF Shear-FFF Steric-FFF Hydrodynamic Lift Forces Capillary Hydrodynamic Fractionation (CHDF) Focusing-FFF Focusing-S-FFF Isoelectric-Focusing-FFF Adhesion-FFF/Potential-Barrier FFF Preparative and Micropreparative FFF SPLITT-FFF Gravitational-SPLITT-FFF (Gr-SPLITT-FFF) Electrical- and Magnetic-SPLITT-FFF Diffusion-SPLITT-FFF Selected Applications of FFF Polymers Synthetic Polymers S-FFF Th-FFF Fl-FFF Biopolymers S-FFF Th-FFF Fl-FFF Other FFF Techniques Colloids Synthetic Colloids S-FFF Th-FFF Fl-FFF Other FFF Techniques Natural Colloids S-FFF Particulate Matter Synthetic Particles S-FFF/Gr-FFF Fl-FFF Natural Particles S-FFF Fl-FFF Other Samples S-FFF Th-FFF Fl-FFF Other FFF Techniques Possibilities and Limits Advantages of FFF Problems and Potential Pitfalls Experimental Artifacts Artifacts Due to Sample Non-idealities/Overloading Solvent Effects Sample–Wall Interactions Field Programming Other Problems Zone Spreading Elution of Non-Spherical Samples Recent Developments Fl-FFF for Organic Solvents FFF Coupled with MALLS Detection Other Fl-FFF Improvements Outlook to the Future Conclusions FFF on the Internet References Capillary Electrophoresis in Polymer Analysis Introduction Mobility and Diffusion Electrophoretic Migration Electroosmotic Flow Modification of Capillary Surfaces Band Broadening Principles of Optimization in Capillary Electrophoresis Influence of pH Effect of Buffer Concentration Type of Buffer Separation of Biopolymers Properties of Sieving Media Migration Theories for DNA Molecules in Capillary Gel Electrophoresis Separation of DNA Separation of Proteins Separation of Synthetic Polyelectrolytes Polystryrenesulfonates Separation of Cationic Polyelectrolytes Other Water-Soluble Polymers Conclusions References Author Index Volumes 101-150 Subject Index

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